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Highest experience reward for killing?
With the number of BG2 specialists here, I think someone will surely know which baddies give you the highest experience rewards in the whole game.
I recall that you get 64K for Firkraag and 50K for Bodhi. So, those two are definitely up there among the highest.
I think you don't get any XP for killing Irenicus, either up in the tree or down in Hell. Demogorgon only gives you quest experience points (and plenty of them), so for the purposes of this question, he doesn't count, either.
Does any monster / bad guy give you more than 64K experience points?